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1 article(s) from Sau, Abhijit

Convergent synthesis of the tetrasaccharide repeating unit of the cell wall lipopolysaccharide of Escherichia coli O40

Abhijit Sau and
Anup Kumar Misra

Beilstein J. Org. Chem. 2012, 8, 2053–2059, doi:10.3762/bjoc.8.230

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Figure 1: Structure of the tetrasaccharide repeating unit of the cell-wall lipopolysaccharide of Escherichia ...

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Figure 2: Structure of the synthesized tetrasaccharide 1 and its synthetic precursors.

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Scheme 1: Synthesis of disaccharide derivative 8. Reagents and conditions: (a) benzyl bromide, NaOH, DMF, roo...

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Scheme 2: Synthesis of disaccharide derivative 9. Reagents and conditions: (a) NIS, HClO₄–SiO₂, MS 4Å, CH₂Cl₂...

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Scheme 3: Synthesis of target tetrasaccharide 1. Reagents and conditions: (a) NIS, HClO₄–SiO₂, CH₂Cl₂, −15 °C...

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Published 22 Nov 2012

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